Information card for entry 7705616

Structure parameters

• Formula: C64 H96 F24 N8 P4 Pd2 Si8
• Calculated formula: C64 H96 F24 N8 P4 Pd2 Si8
• Title of publication: Flexibility and anion exchange of [(X)@Pd₂L₄] cages for recognition of size and charge of polyatomic anions.
• Authors of publication: Lee, Jeyeong; Lim, Sangwoo; Kim, Dongwon; Jung, Ok-Sang; Lee, Young-A
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 42
• Pages of publication: 15002 - 15008
• a: 16.586 ± 0.003 Å
• b: 19.95 ± 0.004 Å
• c: 57.908 ± 0.012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 19161 ± 7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 70
• Hermann-Mauguin space group symbol: F d d d :2
• Hall space group symbol: -F 2uv 2vw
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0949
• Weighted residual factors for significantly intense reflections: 0.2909
• Weighted residual factors for all reflections included in the refinement: 0.2974
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.65 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No