Crystallography Open Database

Information card for entry 7707087

Preview

Coordinates	7707087.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H53 Ag Al F3.5 N3 O3 P3 S
Calculated formula	C34 H53 Ag Al F3.5 N3 O3 P3 S
Title of publication	Formation of an Ag→Al dative bond is avoided in reactions of an alane/tris(phosphine) ligand with monovalent silver.
Authors of publication	Lai, Qingheng; Bhuvanesh, Nattamai; Zhou, Jia; Ozerov, Oleg V.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	17
Pages of publication	5776 - 5778
a	11.3342 ± 0.0013 Å
b	20.425 ± 0.002 Å
c	18.117 ± 0.002 Å
α	90°
β	95.963 ± 0.001°
γ	90°
Cell volume	4171.4 ± 0.8 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0422
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for significantly intense reflections	0.0617
Weighted residual factors for all reflections included in the refinement	0.0666
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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