Information card for entry 7707088

Structure parameters

• Formula: C41.5 H64 Ag Al B11 Cl11 N3 P3
• Calculated formula: C41.5 H64 Ag Al B11 Cl11 N3 P3
• Title of publication: Formation of an Ag→Al dative bond is avoided in reactions of an alane/tris(phosphine) ligand with monovalent silver.
• Authors of publication: Lai, Qingheng; Bhuvanesh, Nattamai; Zhou, Jia; Ozerov, Oleg V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 17
• Pages of publication: 5776 - 5778
• a: 10.6286 ± 0.001 Å
• b: 15.2317 ± 0.0015 Å
• c: 21.256 ± 0.002 Å
• α: 105.088 ± 0.001°
• β: 102.965 ± 0.001°
• γ: 103.394 ± 0.001°
• Cell volume: 3080.2 ± 0.5 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0434
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0624
• Weighted residual factors for all reflections included in the refinement: 0.0681
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No