Information card for entry 7707701

Structure parameters

• Formula: C65 H65.3 Cl3 F7 N4 O1.15 Rh
• Calculated formula: C65 H65.3 Cl3 F7 N4 O1.15 Rh
• Title of publication: Base-promoted perfluoroalkylation of rhodium(III) porphyrin complexes.
• Authors of publication: Fu, Li-Jie; An, Bo-Hsun; Chou, Chih-Hsuan; Chen, Chi-Min; To, Ching Tat
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2021
• Journal volume: 50
• Journal issue: 28
• Pages of publication: 9949 - 9957
• a: 14.8018 ± 0.0008 Å
• b: 29.3344 ± 0.0015 Å
• c: 14.4536 ± 0.0007 Å
• α: 90°
• β: 107.663 ± 0.002°
• γ: 90°
• Cell volume: 5979.9 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.089
• Residual factor for significantly intense reflections: 0.0674
• Weighted residual factors for significantly intense reflections: 0.1916
• Weighted residual factors for all reflections included in the refinement: 0.2062
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No