Crystallography Open Database

Information card for entry 7707702

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Coordinates	7707702.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H63 F7 N4 O Rh
Calculated formula	C64 H63 F7 N4 O Rh
Title of publication	Base-promoted perfluoroalkylation of rhodium(III) porphyrin complexes.
Authors of publication	Fu, Li-Jie; An, Bo-Hsun; Chou, Chih-Hsuan; Chen, Chi-Min; To, Ching Tat
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	28
Pages of publication	9949 - 9957
a	29.171 ± 0.005 Å
b	10.6913 ± 0.0018 Å
c	21.741 ± 0.003 Å
α	90°
β	110.572 ± 0.009°
γ	90°
Cell volume	6348.1 ± 1.8 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.1325
Residual factor for significantly intense reflections	0.0961
Weighted residual factors for significantly intense reflections	0.2483
Weighted residual factors for all reflections included in the refinement	0.2857
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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