Information card for entry 7715250

Structure parameters

• Formula: C139 H284 Al6 Si24
• Calculated formula: C139 H284 Al6 Si24
• Title of publication: Hexadentate poly-Lewis acids based on the bowl-shaped tribenzotriquinacene.
• Authors of publication: Franke, Maurice; Klingsiek, Maximilian J.; Buth, Julian; Lamm, Jan-Hendrik; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 7751 - 7762
• a: 17.4659 ± 0.0005 Å
• b: 21.6812 ± 0.0006 Å
• c: 26.9593 ± 0.0008 Å
• α: 105.168 ± 0.002°
• β: 93.414 ± 0.002°
• γ: 105.343 ± 0.002°
• Cell volume: 9410.8 ± 0.5 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1088
• Residual factor for significantly intense reflections: 0.0755
• Weighted residual factors for significantly intense reflections: 0.1703
• Weighted residual factors for all reflections included in the refinement: 0.1872
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No