Information card for entry 7715251

Structure parameters

• Formula: C181 H352 Al6 P6 Si27
• Calculated formula: C151 H322 Al6 P6 Si27
• Title of publication: Hexadentate poly-Lewis acids based on the bowl-shaped tribenzotriquinacene.
• Authors of publication: Franke, Maurice; Klingsiek, Maximilian J.; Buth, Julian; Lamm, Jan-Hendrik; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 7751 - 7762
• a: 25.0396 ± 0.0004 Å
• b: 25.2861 ± 0.0005 Å
• c: 28.1063 ± 0.0005 Å
• α: 95.762 ± 0.001°
• β: 106.883 ± 0.002°
• γ: 118.836 ± 0.002°
• Cell volume: 14290.2 ± 0.6 ų
• Cell temperature: 99.98 ± 0.1 K
• Ambient diffraction temperature: 99.98 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1115
• Residual factor for significantly intense reflections: 0.0831
• Weighted residual factors for significantly intense reflections: 0.2255
• Weighted residual factors for all reflections included in the refinement: 0.2542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No