Information card for entry 7715666

Structure parameters

• Formula: C30 H90 N6 O3 Si8 Yb2
• Calculated formula: C30 H90 N6 O3 Si8 Yb2
• Title of publication: Formation of <i>N</i>,<i>N</i>,<i>N</i>',<i>N</i>'-tetramethylethylenediamine <i>via</i> coupling of the two charge reversed C-N bonds of Me₃NO in the presence of an Eu(II) bis(trimethylsilyl)amide complex.
• Authors of publication: Li, Yangjuan; Gong, Yu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5342 - 5345
• a: 10.661 ± 0.0004 Å
• b: 11.9772 ± 0.0005 Å
• c: 12.3171 ± 0.0006 Å
• α: 118.634 ± 0.005°
• β: 102.46 ± 0.004°
• γ: 90.275 ± 0.004°
• Cell volume: 1337.11 ± 0.12 ų
• Cell temperature: 180 ± 0.1 K
• Ambient diffraction temperature: 180 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No