Information card for entry 7717313

Structure parameters

• Formula: C140 H234 N16 Np4 O21
• Calculated formula: C140 H234 N16 Np4 O21
• Title of publication: Electroanalytical characterization of Np(VI)/Np(V) redox in a pentadentate ligand environment and stabilization of [Np^VO₂]⁺ by hydrogen bonding.
• Authors of publication: Mikeska, Emily R.; Curry, T. Davis; Wilson, Richard E.; Blakemore, James D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 48
• Pages of publication: 19126 - 19142
• a: 9.9804 ± 0.0007 Å
• b: 18.0918 ± 0.0013 Å
• c: 21.0492 ± 0.0015 Å
• α: 93.77 ± 0.001°
• β: 98.483 ± 0.001°
• γ: 94.106 ± 0.001°
• Cell volume: 3738.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0981
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.0846
• Weighted residual factors for all reflections included in the refinement: 0.0968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.13
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No