Information card for entry 7717314

Structure parameters

• Formula: C70 H120 N8 Np2 O11
• Calculated formula: C70 H120 N8 Np2 O11
• Title of publication: Electroanalytical characterization of Np(VI)/Np(V) redox in a pentadentate ligand environment and stabilization of [Np^VO₂]⁺ by hydrogen bonding.
• Authors of publication: Mikeska, Emily R.; Curry, T. Davis; Wilson, Richard E.; Blakemore, James D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2024
• Journal volume: 53
• Journal issue: 48
• Pages of publication: 19126 - 19142
• a: 9.9521 ± 0.0004 Å
• b: 18.0582 ± 0.0008 Å
• c: 21.1643 ± 0.0009 Å
• α: 93.562 ± 0.001°
• β: 97.981 ± 0.001°
• γ: 94.439 ± 0.001°
• Cell volume: 3745.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0879
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.1157
• Weighted residual factors for all reflections included in the refinement: 0.1308
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No