Crystallography Open Database

Information card for entry 7717664

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Coordinates	7717664.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H42 O3 Si2 W
Calculated formula	C24 H42 O3 Si2 W
Title of publication	A hydrogen-bridged bis(silylene) complex as a platform for small molecule activation <i>via</i> adjacent metal-ligand cooperation.
Authors of publication	Hashimoto, Hisako; Matsuo, Satomi; Odagiri, Yuto; Tobita, Hiromi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2025
Journal volume	54
Journal issue	3
Pages of publication	915 - 919
a	26.4496 ± 0.0013 Å
b	15.6024 ± 0.0011 Å
c	15.888 ± 0.0009 Å
α	90°
β	125.361 ± 0.0012°
γ	90°
Cell volume	5347 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0293
Residual factor for significantly intense reflections	0.0263
Weighted residual factors for significantly intense reflections	0.0643
Weighted residual factors for all reflections included in the refinement	0.066
Goodness-of-fit parameter for all reflections included in the refinement	1.118
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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