Information card for entry 7717665

Structure parameters

• Formula: C29 H48 O3 Si2 W
• Calculated formula: C29 H48 O3 Si2 W
• Title of publication: A hydrogen-bridged bis(silylene) complex as a platform for small molecule activation <i>via</i> adjacent metal-ligand cooperation.
• Authors of publication: Hashimoto, Hisako; Matsuo, Satomi; Odagiri, Yuto; Tobita, Hiromi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 3
• Pages of publication: 915 - 919
• a: 17.1114 ± 0.0006 Å
• b: 10.5152 ± 0.0005 Å
• c: 16.394 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2949.8 ± 0.2 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.0666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.173
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No