Information card for entry 7717666

Structure parameters

• Formula: C33 H52 N2 O2 Si2 W
• Calculated formula: C33 H52.5 N2 O2 Si2 W
• Title of publication: A hydrogen-bridged bis(silylene) complex as a platform for small molecule activation <i>via</i> adjacent metal-ligand cooperation.
• Authors of publication: Hashimoto, Hisako; Matsuo, Satomi; Odagiri, Yuto; Tobita, Hiromi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 3
• Pages of publication: 915 - 919
• a: 14.241 ± 0.0002 Å
• b: 33.3455 ± 0.0006 Å
• c: 14.4026 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6839.4 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0667
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for significantly intense reflections: 0.1119
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.375
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No