Information card for entry 7718102

Structure parameters

• Formula: C4.51 H5.43 Cl0.1 F1.23 N0.77 O0.41 Os0.15 P0.21
• Calculated formula: C4.51231 H5.42646 Cl0.102308 F1.23231 N0.769231 O0.41 Os0.153846 P0.205385
• Title of publication: Synthesis of [Os(bpy)2(py)(OH2)](PF6)x substituted pyridine complexes; characterization of a singly bridged H3O2− ligand
• Authors of publication: Sun, Jiangtian; Sun, Jingwen; Jolly, Brandon J.; Riu, Martin-Louis Y.; Kerr, Tyler A.; Lai, Yi-An; Pung, Michael J.; Liu, Chong; Nava, Matthew
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 12
• Pages of publication: 5109 - 5118
• a: 17.1152 ± 0.001 Å
• b: 8.7658 ± 0.0005 Å
• c: 22.3304 ± 0.0014 Å
• α: 90°
• β: 102.552 ± 0.002°
• γ: 90°
• Cell volume: 3270.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0334
• Weighted residual factors for significantly intense reflections: 0.0562
• Weighted residual factors for all reflections included in the refinement: 0.0628
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No