Information card for entry 7718103

Structure parameters

• Formula: C62.4 H77.8 F30 N12 O4 Os2 P5
• Calculated formula: C62.4 H77.8 F30 N12 O4 Os2 P5
• Title of publication: Synthesis of [Os(bpy)2(py)(OH2)](PF6)x substituted pyridine complexes; characterization of a singly bridged H3O2− ligand
• Authors of publication: Sun, Jiangtian; Sun, Jingwen; Jolly, Brandon J.; Riu, Martin-Louis Y.; Kerr, Tyler A.; Lai, Yi-An; Pung, Michael J.; Liu, Chong; Nava, Matthew
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 12
• Pages of publication: 5109 - 5118
• a: 12.0421 ± 0.0005 Å
• b: 13.5806 ± 0.0006 Å
• c: 14.2226 ± 0.0006 Å
• α: 62.14 ± 0.001°
• β: 83.454 ± 0.002°
• γ: 69.784 ± 0.001°
• Cell volume: 1926.51 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.0358
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0828
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No