Information card for entry 7718685

Structure parameters

• Formula: C74 H82 N6 O6
• Calculated formula: C74 H82 N6 O6
• Title of publication: New mononuclear Dy(III) complex based on a calix[4]arene ligand with two appended salicylideneamine groups decorated with azophenyl fragments: synthesis, crystalline assembly and slow magnetic relaxation behavior.
• Authors of publication: Strelnikova, Iuliia V.; Iova, Angelina A.; Ovsyannikov, Alexander S.; Islamov, Daut R.; Litvonov, Igor A.; Lazarenko, Vladimir A.; Kulikova, Elizaveta S.; Bogomyakov, Artem S.; Lin, Meijin; Kiiamov, Airat G.; Solovieva, Svetlana E.; Antipin, Igor S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 24
• Pages of publication: 9584 - 9593
• a: 10.544 ± 0.0012 Å
• b: 16.2534 ± 0.0019 Å
• c: 19.985 ± 0.002 Å
• α: 90.635 ± 0.004°
• β: 102.105 ± 0.004°
• γ: 108.609 ± 0.004°
• Cell volume: 3162.4 ± 0.6 ų
• Cell temperature: 105 ± 2 K
• Ambient diffraction temperature: 105 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.0804
• Weighted residual factors for significantly intense reflections: 0.1918
• Weighted residual factors for all reflections included in the refinement: 0.2091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No