Information card for entry 7718686

Structure parameters

• Formula: C75 H87 Dy N6 O9
• Calculated formula: C75 H87 Dy N6 O9
• Title of publication: New mononuclear Dy(III) complex based on a calix[4]arene ligand with two appended salicylideneamine groups decorated with azophenyl fragments: synthesis, crystalline assembly and slow magnetic relaxation behavior.
• Authors of publication: Strelnikova, Iuliia V.; Iova, Angelina A.; Ovsyannikov, Alexander S.; Islamov, Daut R.; Litvonov, Igor A.; Lazarenko, Vladimir A.; Kulikova, Elizaveta S.; Bogomyakov, Artem S.; Lin, Meijin; Kiiamov, Airat G.; Solovieva, Svetlana E.; Antipin, Igor S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 24
• Pages of publication: 9584 - 9593
• a: 19.127 ± 0.004 Å
• b: 13.967 ± 0.003 Å
• c: 26.635 ± 0.005 Å
• α: 90°
• β: 96.86 ± 0.03°
• γ: 90°
• Cell volume: 7065 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1809
• Residual factor for significantly intense reflections: 0.1127
• Weighted residual factors for significantly intense reflections: 0.2708
• Weighted residual factors for all reflections included in the refinement: 0.3244
• Goodness-of-fit parameter for all reflections included in the refinement: 1.22
• Diffraction radiation wavelength: 0.7517 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No