Information card for entry 7718912

Structure parameters

• Formula: C35 H91 Ge9 Ir O2 Si13
• Calculated formula: C35 H91 Ge9 Ir O2 Si13
• Title of publication: Oxidative addition of Si-H bonds to metal-decorated Zintl clusters [Hyp₃Ge₉Ir(CO)PR₃] (R = Ph, ^<i>p</i>tolyl, Me).
• Authors of publication: Willeit, Nicole S.; Kratky, Tim; Hlukhyy, Viktor; Günther, Sebastian; Fässler, Thomas F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 28
• Pages of publication: 10973 - 10983
• a: 26.26 ± 0.005 Å
• b: 14.83 ± 0.003 Å
• c: 18.79 ± 0.004 Å
• α: 90°
• β: 100.7 ± 0.03°
• γ: 90°
• Cell volume: 7190 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.126
• Residual factor for significantly intense reflections: 0.0815
• Weighted residual factors for significantly intense reflections: 0.1919
• Weighted residual factors for all reflections included in the refinement: 0.212
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No