Information card for entry 7719122

Structure parameters

• Formula: C117 H240 Ce4 N12 O32 Si8
• Calculated formula: C117 H239 Ce4 N12 O32 Si8
• Title of publication: Stepwise azido transfer to cerous tris(<i>tert</i>-butoxy)siloxide <i>via</i> trans-silylation with Me₃SiN₃.
• Authors of publication: Friedrich, Jochen; Riedmaier, Jonas; Maichle-Mössmer, Cäcilia; Anwander, Reiner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 32
• Pages of publication: 12141 - 12144
• a: 34.146 ± 0.0011 Å
• b: 24.5317 ± 0.0008 Å
• c: 19.3428 ± 0.0006 Å
• α: 90°
• β: 95.477 ± 0.001°
• γ: 90°
• Cell volume: 16128.7 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0349
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0485
• Weighted residual factors for all reflections included in the refinement: 0.0546
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No