Information card for entry 7719208

Structure parameters

• Formula: C51 H39 Cl2 N5 P2
• Calculated formula: C51 H39 Cl2 N5 P2
• Title of publication: A new class of ligand derived from the reactions of bis(dialkylphosphino)amines and 9-diazofluorene: preparation, structure and reactivity.
• Authors of publication: Laprade, Matthew J. J.; Robertson, Katherine N.; Clyburne, Jason A. C.; Kozak, Christopher M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 29
• Pages of publication: 11382 - 11397
• a: 10.4341 ± 0.001 Å
• b: 11.7915 ± 0.0012 Å
• c: 18.6856 ± 0.0018 Å
• α: 96.945 ± 0.001°
• β: 91.378 ± 0.001°
• γ: 111.064 ± 0.001°
• Cell volume: 2123.9 ± 0.4 ų
• Cell temperature: 125 ± 2 K
• Ambient diffraction temperature: 125 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No