Information card for entry 7719209

Structure parameters

• Formula: C62 H60 N5 Na O3 P2
• Calculated formula: C62 H60 N5 Na O3 P2
• Title of publication: A new class of ligand derived from the reactions of bis(dialkylphosphino)amines and 9-diazofluorene: preparation, structure and reactivity.
• Authors of publication: Laprade, Matthew J. J.; Robertson, Katherine N.; Clyburne, Jason A. C.; Kozak, Christopher M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 29
• Pages of publication: 11382 - 11397
• a: 10.72595 ± 0.00014 Å
• b: 12.93932 ± 0.00018 Å
• c: 20.3684 ± 0.0003 Å
• α: 106.175 ± 0.0012°
• β: 102.187 ± 0.0011°
• γ: 94.7288 ± 0.0011°
• Cell volume: 2623.55 ± 0.07 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1163
• Weighted residual factors for all reflections included in the refinement: 0.1235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No