Information card for entry 7719210

Structure parameters

• Formula: C37 H29 N3 O P2
• Calculated formula: C37 H29 N3 O P2
• Title of publication: A new class of ligand derived from the reactions of bis(dialkylphosphino)amines and 9-diazofluorene: preparation, structure and reactivity.
• Authors of publication: Laprade, Matthew J. J.; Robertson, Katherine N.; Clyburne, Jason A. C.; Kozak, Christopher M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 29
• Pages of publication: 11382 - 11397
• a: 8.812 ± 0.003 Å
• b: 12.958 ± 0.005 Å
• c: 13.777 ± 0.005 Å
• α: 87.987 ± 0.005°
• β: 79.194 ± 0.005°
• γ: 71.304 ± 0.005°
• Cell volume: 1463.2 ± 0.9 ų
• Cell temperature: 125 ± 2 K
• Ambient diffraction temperature: 125 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1497
• Residual factor for significantly intense reflections: 0.0804
• Weighted residual factors for significantly intense reflections: 0.1914
• Weighted residual factors for all reflections included in the refinement: 0.2258
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No