Information card for entry 7719509

Structure parameters

• Formula: C114 H93 O3 P8 Rh4
• Calculated formula: C114 H92 O3 P8 Rh4
• Title of publication: Sodium phosphaethynolate as P-source for the synthesis of molecular rhodium phosphides: an exploratory study.
• Authors of publication: Li, Zhongshu; Borger, Jaap E.; Gianetti, Thomas L.; Müller, Fabian; Pribanic, Bruno; Coburger, Peter; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 45
• Pages of publication: 16718 - 16726
• a: 14.5881 ± 0.0003 Å
• b: 15.3992 ± 0.0004 Å
• c: 23.9098 ± 0.0004 Å
• α: 88.72 ± 0.002°
• β: 74.986 ± 0.002°
• γ: 76.727 ± 0.002°
• Cell volume: 5045.3 ± 0.2 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.0871
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No