Information card for entry 7719510

Structure parameters

• Formula: C87 H72 N6 Na O3 P5 Rh2
• Calculated formula: C87 H72 N6 Na O3 P5 Rh2
• Title of publication: Sodium phosphaethynolate as P-source for the synthesis of molecular rhodium phosphides: an exploratory study.
• Authors of publication: Li, Zhongshu; Borger, Jaap E.; Gianetti, Thomas L.; Müller, Fabian; Pribanic, Bruno; Coburger, Peter; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 45
• Pages of publication: 16718 - 16726
• a: 15.2977 ± 0.0004 Å
• b: 18.7962 ± 0.0005 Å
• c: 26.1377 ± 0.0008 Å
• α: 90°
• β: 90.337 ± 0.001°
• γ: 90°
• Cell volume: 7515.5 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100.02 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0901
• Weighted residual factors for all reflections included in the refinement: 0.0944
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No