Information card for entry 7719552

Structure parameters

• Formula: C65 H63 Cl4 N8 O4.5 Os P
• Calculated formula: C65 H63 Cl4 N8 O4.5 Os P
• Title of publication: Reaction of an osmium(VI) nitrido complex with enamines generated <i>in situ</i> from ketones and anilines.
• Authors of publication: Wang, Lei; Wang, Li-Xin; Liu, Zhao-Long; Xu, Fang; Qi, Rui-Yue; Man, Wai-Lun; Xiang, Jing; Liu, Ji-Yan; Lau, Tai-Chu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 37
• Pages of publication: 14052 - 14058
• a: 12.801 ± 0.0008 Å
• b: 16.1249 ± 0.001 Å
• c: 17.2027 ± 0.0012 Å
• α: 99.594 ± 0.003°
• β: 106.007 ± 0.002°
• γ: 106.386 ± 0.002°
• Cell volume: 3157.4 ± 0.4 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No