Information card for entry 7719553

Structure parameters

• Formula: C53.5 H43 N8 O5 Os P
• Calculated formula: C53.5 H43 N8 O5 Os P
• Title of publication: Reaction of an osmium(VI) nitrido complex with enamines generated <i>in situ</i> from ketones and anilines.
• Authors of publication: Wang, Lei; Wang, Li-Xin; Liu, Zhao-Long; Xu, Fang; Qi, Rui-Yue; Man, Wai-Lun; Xiang, Jing; Liu, Ji-Yan; Lau, Tai-Chu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2025
• Journal volume: 54
• Journal issue: 37
• Pages of publication: 14052 - 14058
• a: 13.3204 ± 0.0003 Å
• b: 16.0179 ± 0.0004 Å
• c: 23.9832 ± 0.0008 Å
• α: 90°
• β: 103.161 ± 0.002°
• γ: 90°
• Cell volume: 4982.8 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0285
• Weighted residual factors for significantly intense reflections: 0.0699
• Weighted residual factors for all reflections included in the refinement: 0.0722
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No