Information card for entry 7719940

Structure parameters

• Formula: C40 H60 Ir4 K23 O156 Si4 W40
• Calculated formula: C40 H60 Ir4 K23 O156 Si4 W40
• Title of publication: Reaction of a Cp*Ir(III) Cation with mono-and di-lacunary Keggintype heterpolytungstates, and dimer of hexa-lacunary Dawsontype phosphopolytungstate
• Authors of publication: Sugiarto, Sugiarto; Shinogi, Jun; Ebied, Sherif E.; Hong, Dachao; Kon, Yoshihiro; Sadakane, Masahiro
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• a: 31.071 ± 0.003 Å
• b: 31.071 ± 0.003 Å
• c: 15.191 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14665 ± 3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1343
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No