Information card for entry 7719941

Structure parameters

• Formula: C20 Cl Ir2 K5 O52.6 Si W11
• Calculated formula: C20 Cl Ir2 K5 O52.6 Si W11
• Title of publication: Reaction of a Cp*Ir(III) Cation with mono-and di-lacunary Keggintype heterpolytungstates, and dimer of hexa-lacunary Dawsontype phosphopolytungstate
• Authors of publication: Sugiarto, Sugiarto; Shinogi, Jun; Ebied, Sherif E.; Hong, Dachao; Kon, Yoshihiro; Sadakane, Masahiro
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• a: 22.3953 ± 0.0016 Å
• b: 11.5329 ± 0.0008 Å
• c: 27.827 ± 0.002 Å
• α: 90°
• β: 104.913 ± 0.001°
• γ: 90°
• Cell volume: 6945.2 ± 0.9 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0722
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1405
• Weighted residual factors for all reflections included in the refinement: 0.1422
• Goodness-of-fit parameter for all reflections included in the refinement: 1.257
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No