Information card for entry 7719943

Structure parameters

• Formula: C40 H0 Ir4 K29.8 O257.31 P8 W48.62
• Calculated formula: C40 Ir4 K29.8 O257.296 P8 W48.6166
• Title of publication: Reaction of a Cp*Ir(III) Cation with mono-and di-lacunary Keggintype heterpolytungstates, and dimer of hexa-lacunary Dawsontype phosphopolytungstate
• Authors of publication: Sugiarto, Sugiarto; Shinogi, Jun; Ebied, Sherif E.; Hong, Dachao; Kon, Yoshihiro; Sadakane, Masahiro
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• a: 17.5552 ± 0.0016 Å
• b: 22.843 ± 0.002 Å
• c: 23.043 ± 0.002 Å
• α: 65.373 ± 0.001°
• β: 67.697 ± 0.001°
• γ: 85.608 ± 0.001°
• Cell volume: 7735 ± 1.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0453
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0836
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No