Information card for entry 7719942

Structure parameters

• Formula: C20 Cl Ir2 K3.4 O47.63 P W11
• Calculated formula: C20 Cl Ir2 K3.4 O47.64 P W11
• Title of publication: Reaction of a Cp*Ir(III) Cation with mono-and di-lacunary Keggintype heterpolytungstates, and dimer of hexa-lacunary Dawsontype phosphopolytungstate
• Authors of publication: Sugiarto, Sugiarto; Shinogi, Jun; Ebied, Sherif E.; Hong, Dachao; Kon, Yoshihiro; Sadakane, Masahiro
• Journal of publication: Dalton Transactions
• Year of publication: 2025
• a: 35.1781 ± 0.0013 Å
• b: 35.1781 ± 0.0013 Å
• c: 11.3965 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14103.2 ± 1 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.1055
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No