Information card for entry 1100576

Structure parameters

• Formula: C22 H48 Li2 N2 O3 Si
• Calculated formula: C58 H130 Li4 N4 O5 Si
• Title of publication: Synthese eines Titana-Oxacyclohexanringes durch kontrollierte Ringöffnung von Tetrahydrofuran. Kristallstrukturen von [Ti(CH~2~)~4~O{Me~2~Si(NBut)~2~}]~2~, [TiCl{Me~2~Si(NBut)~2~}]~3~(μ~3~-O)(μ~3~-Cl) und [Li~2~(THF)~3~{Me~2~Si(NBut)~2~}]
• Authors of publication: Mommertz, Andreas; Leo, Roland; Massa, Werner; Harms, Klaus; Dehnicke, Kurt
• Journal of publication: Zeitschrift fuer Anorganische und Allgemeine Chemie
• Year of publication: 1998
• Journal volume: 624
• Journal issue: 10
• Pages of publication: 1647 - 1652
• a: 11.509 ± 0.0008 Å
• b: 15.5891 ± 0.0013 Å
• c: 16.4206 ± 0.0004 Å
• α: 90°
• β: 95.697 ± 0.005°
• γ: 90°
• Cell volume: 2931.55 ų
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No