Information card for entry 1100798

Structure parameters

• Formula: C18 H36 N2 Si2 Zr
• Calculated formula: C18 H36 N2 Si2 Zr
• Title of publication: Insertion Reactions into the Metal‒Alkyl and Metal‒Amido Bonds of 1,3-Di(silyl-η-amido)cyclopentadienyl Titanium and Zirconium Complexes
• Authors of publication: Cano, Jesús; Sudupe, María; Royo, Pascual; Mosquera, Marta E. G.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 10
• Pages of publication: 2424 - 2432
• a: 11.3691 ± 0.0015 Å
• b: 13.9028 ± 0.0009 Å
• c: 15.137 ± 0.002 Å
• α: 90°
• β: 108.131 ± 0.012°
• γ: 90°
• Cell volume: 2273.8 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No