Information card for entry 1100799

Structure parameters

• Formula: C33 H49 N3 Si2 Zr
• Calculated formula: C33 H49 N3 Si2 Zr
• Title of publication: Insertion Reactions into the Metal‒Alkyl and Metal‒Amido Bonds of 1,3-Di(silyl-η-amido)cyclopentadienyl Titanium and Zirconium Complexes
• Authors of publication: Cano, Jesús; Sudupe, María; Royo, Pascual; Mosquera, Marta E. G.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 10
• Pages of publication: 2424 - 2432
• a: 11.119 ± 0.002 Å
• b: 19.43 ± 0.004 Å
• c: 15.805 ± 0.002 Å
• α: 90°
• β: 106.355 ± 0.011°
• γ: 90°
• Cell volume: 3276.4 ± 1 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1359
• Residual factor for significantly intense reflections: 0.0636
• Weighted residual factors for significantly intense reflections: 0.121
• Weighted residual factors for all reflections included in the refinement: 0.1446
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No