Information card for entry 1100800

Structure parameters

• Formula: C36 H54 N4 Si2 Ti
• Calculated formula: C36 H54 N4 Si2 Ti
• Title of publication: Insertion Reactions into the Metal–Alkyl and Metal–Amido Bonds of 1,3-Di(silyl-η-amido)cyclopentadienyl Titanium and Zirconium Complexes
• Authors of publication: Cano, Jesús; Sudupe, María; Royo, Pascual; Mosquera, Marta E. G.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 10
• Pages of publication: 2424 - 2432
• a: 9.7722 ± 0.001 Å
• b: 11.3369 ± 0.0004 Å
• c: 17.0066 ± 0.0016 Å
• α: 98.372 ± 0.006°
• β: 102.866 ± 0.01°
• γ: 99.863 ± 0.007°
• Cell volume: 1776.2 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1097
• Residual factor for significantly intense reflections: 0.0614
• Weighted residual factors for significantly intense reflections: 0.1466
• Weighted residual factors for all reflections included in the refinement: 0.1654
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No