Crystallography Open Database

Information card for entry 1100899

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Coordinates	1100899.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35.5 H69 Ge N2 P2 Si4
Calculated formula	C35 H68 Ge N2 P2 Si4
Title of publication	An Intramolecularly Base-Stabilized Diphosphagermylene and Two Unusual Germanium(II) Ate Complexes: A Structural, NMR, and DFT Study
Authors of publication	Izod, Keith; McFarlane, William; Allen, Ben; Clegg, William; Harrington, Ross W.
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	9
Pages of publication	2157 - 2167
a	11.4596 ± 0.0005 Å
b	12.0029 ± 0.0005 Å
c	16.3524 ± 0.0007 Å
α	78.569 ± 0.001°
β	89.576 ± 0.001°
γ	75.536 ± 0.001°
Cell volume	2132.65 ± 0.16 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0299
Residual factor for significantly intense reflections	0.0268
Weighted residual factors for significantly intense reflections	0.0755
Weighted residual factors for all reflections included in the refinement	0.0776
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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