Information card for entry 1100900

Structure parameters

• Formula: C44 H92 Ge I2 Li2 N2 O3 P2 Si4
• Calculated formula: C44 H92 Ge I2 Li2 N2 O3 P2 Si4
• Title of publication: An Intramolecularly Base-Stabilized Diphosphagermylene and Two Unusual Germanium(II) Ate Complexes: A Structural, NMR, and DFT Study
• Authors of publication: Izod, Keith; McFarlane, William; Allen, Ben; Clegg, William; Harrington, Ross W.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 9
• Pages of publication: 2157 - 2167
• a: 48.748 ± 0.003 Å
• b: 11.2312 ± 0.0006 Å
• c: 11.141 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6099.7 ± 0.6 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 9
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0581
• Residual factor for significantly intense reflections: 0.0476
• Weighted residual factors for significantly intense reflections: 0.0965
• Weighted residual factors for all reflections included in the refinement: 0.0998
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No