Information card for entry 1100901

Structure parameters

• Formula: C48 H93 Ge K N3 P3 Si6
• Calculated formula: C48 H93 Ge K N3 P3 Si6
• Title of publication: An Intramolecularly Base-Stabilized Diphosphagermylene and Two Unusual Germanium(II) Ate Complexes: A Structural, NMR, and DFT Study
• Authors of publication: Izod, Keith; McFarlane, William; Allen, Ben; Clegg, William; Harrington, Ross W.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 9
• Pages of publication: 2157 - 2167
• a: 23.4873 ± 0.0005 Å
• b: 23.4873 ± 0.0005 Å
• c: 23.4873 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12956.8 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 205
• Hermann-Mauguin space group symbol: P a -3
• Hall space group symbol: -P 2ac 2ab 3
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.1185
• Weighted residual factors for all reflections included in the refinement: 0.1358
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No