Information card for entry 1505412

Structure parameters

• Formula: C36 H66 O11 S Si2
• Calculated formula: C36 H66 O11 S Si2
• SMILES: S(=O)(=O)(CC[C@H](O[Si](C(C)(C)C)(C)C)[C@@H](OC)C[C@H](O)[C@H](O)[C@@]1(O[C@@H]([C@@H]([C@H](O[Si](C(C)(C)C)(C)C)[C@H]1C)C)CC(=O)OC)O)c1ccccc1
• Title of publication: Lactol-directed osmylation. Stereodivergent synthesis of four C-19,20 apoptolidin diols from a single allylic hemiacetal.
• Authors of publication: Kim, Youngsoon; Fuchs, Philip L.
• Journal of publication: Organic letters
• Year of publication: 2007
• Journal volume: 9
• Journal issue: 13
• Pages of publication: 2445 - 2448
• a: 11.0209 ± 0.0002 Å
• b: 12.2273 ± 0.0002 Å
• c: 31.3304 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4221.95 ± 0.12 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.095
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No