Information card for entry 1505413

Structure parameters

• Formula: C38 H66 O12 S Si2
• Calculated formula: C38 H66 O12 S Si2
• SMILES: S(=O)(=O)(CC[C@H](O[Si](C(C)(C)C)(C)C)[C@@H](OC)C[C@@H]1OC(=O)O[C@H]1[C@@]1(O[C@@H]([C@@H]([C@H](O[Si](C(C)(C)C)(C)C)[C@H]1C)C)CC(=O)OC)OC)c1ccccc1
• Title of publication: Lactol-directed osmylation. Stereodivergent synthesis of four C-19,20 apoptolidin diols from a single allylic hemiacetal.
• Authors of publication: Kim, Youngsoon; Fuchs, Philip L.
• Journal of publication: Organic letters
• Year of publication: 2007
• Journal volume: 9
• Journal issue: 13
• Pages of publication: 2445 - 2448
• a: 7.292 ± 0.0004 Å
• b: 17.7683 ± 0.0017 Å
• c: 17.7243 ± 0.0011 Å
• α: 90°
• β: 98.805 ± 0.004°
• γ: 90°
• Cell volume: 2269.4 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.091
• Residual factor for significantly intense reflections: 0.088
• Weighted residual factors for significantly intense reflections: 0.181
• Weighted residual factors for all reflections included in the refinement: 0.182
• Goodness-of-fit parameter for all reflections included in the refinement: 1.213
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MO-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No