Information card for entry 1506044

Structure parameters

• Formula: C23 H25 N O4 S
• Calculated formula: C23 H25 N O4 S
• SMILES: S(=O)(=O)([C@H]1C(=O)N(C(=O)[C@H]2[C@@H]1CCCC2)Cc1ccccc1)c1ccc(cc1)C.S(=O)(=O)([C@@H]1C(=O)N(C(=O)[C@@H]2[C@H]1CCCC2)Cc1ccccc1)c1ccc(cc1)C
• Title of publication: Efficient synthesis of fused bicyclic glutarimides. Its application to (+/-)-alloyohimbane and louisianin D.
• Authors of publication: Chen, Hung-Wei; Hsu, Ru-Ting; Chang, Meng-Yang; Chang, Nein-Chen
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 14
• Pages of publication: 3033 - 3035
• a: 8.6243 ± 0.0011 Å
• b: 12.1688 ± 0.0016 Å
• c: 20.438 ± 0.003 Å
• α: 90°
• β: 100.164 ± 0.003°
• γ: 90°
• Cell volume: 2111.3 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0584
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1166
• Weighted residual factors for all reflections included in the refinement: 0.129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No