Information card for entry 1506045

Structure parameters

• Formula: C22 H23 N O4 S
• Calculated formula: C22 H23 N O4 S
• SMILES: S(=O)(=O)([C@@H]1C(=O)N(C(=O)[C@@H]2[C@H]1CCC2)Cc1ccccc1)c1ccc(cc1)C.S(=O)(=O)([C@H]1C(=O)N(C(=O)[C@H]2[C@@H]1CCC2)Cc1ccccc1)c1ccc(cc1)C
• Title of publication: Efficient synthesis of fused bicyclic glutarimides. Its application to (+/-)-alloyohimbane and louisianin D.
• Authors of publication: Chen, Hung-Wei; Hsu, Ru-Ting; Chang, Meng-Yang; Chang, Nein-Chen
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 14
• Pages of publication: 3033 - 3035
• a: 19.552 ± 0.002 Å
• b: 7.7459 ± 0.0008 Å
• c: 13.2549 ± 0.0014 Å
• α: 90°
• β: 97.737 ± 0.002°
• γ: 90°
• Cell volume: 1989.2 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0753
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.1471
• Weighted residual factors for all reflections included in the refinement: 0.1678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No