Information card for entry 1508185

Structure parameters

• Formula: C79 H83 N8 O4 Si2 U2
• Calculated formula: C79 H83 N8 O4 Si2 U2
• Title of publication: Strongly coupled binuclear uranium-oxo complexes from uranyl oxo rearrangement and reductive silylation.
• Authors of publication: Arnold, Polly L.; Jones, Guy M.; Odoh, Samuel O.; Schreckenbach, Georg; Magnani, Nicola; Love, Jason B.
• Journal of publication: Nature chemistry
• Year of publication: 2012
• Journal volume: 4
• Journal issue: 3
• Pages of publication: 221 - 227
• a: 15.465 ± 0.0003 Å
• b: 24.4171 ± 0.0006 Å
• c: 20.7529 ± 0.0005 Å
• α: 90°
• β: 101.073 ± 0.002°
• γ: 90°
• Cell volume: 7690.6 ± 0.3 ų
• Cell temperature: 171 ± 2 K
• Ambient diffraction temperature: 171 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0914
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.1049
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No