Information card for entry 1508186

Structure parameters

• Formula: C65 H90 N8 O12 Si U3
• Calculated formula: C65 H90 N8 O12 Si U3
• Title of publication: Strongly coupled binuclear uranium-oxo complexes from uranyl oxo rearrangement and reductive silylation.
• Authors of publication: Arnold, Polly L.; Jones, Guy M.; Odoh, Samuel O.; Schreckenbach, Georg; Magnani, Nicola; Love, Jason B.
• Journal of publication: Nature chemistry
• Year of publication: 2012
• Journal volume: 4
• Journal issue: 3
• Pages of publication: 221 - 227
• a: 14.1406 ± 0.0006 Å
• b: 14.7186 ± 0.0008 Å
• c: 18.347 ± 0.0011 Å
• α: 86.724 ± 0.005°
• β: 77.931 ± 0.004°
• γ: 77.425 ± 0.004°
• Cell volume: 3644.3 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0625
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.0958
• Weighted residual factors for all reflections included in the refinement: 0.1049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No