Information card for entry 1513686

Structure parameters

• Formula: C123.5 H151.5 N2 O6 Se3.86 U2
• Calculated formula: C123.5 H151.5 N2 O6 Se3.8622 U2
• Title of publication: Reactivity of uranium(iv) bridged chalcogenido complexes UIV‒E‒UIV (E = S, Se) with elemental sulfur and selenium: synthesis of polychalcogenido-bridged uranium complexes
• Authors of publication: Franke, Sebastian M.; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Chemical Science
• Year of publication: 2014
• Journal volume: 5
• Journal issue: 3
• Pages of publication: 942
• a: 11.2872 ± 0.0008 Å
• b: 16.8161 ± 0.0012 Å
• c: 28.943 ± 0.002 Å
• α: 85.729 ± 0.002°
• β: 87.925 ± 0.002°
• γ: 89.368 ± 0.002°
• Cell volume: 5474.5 ± 0.7 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0379
• Residual factor for significantly intense reflections: 0.0296
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.0789
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No