Information card for entry 1513687

Structure parameters

• Formula: C130 H164 N2 O8 Se4.11 U2
• Calculated formula: C130 H164 N2 O8 Se4.11 U2
• Title of publication: Reactivity of uranium(iv) bridged chalcogenido complexes UIV‒E‒UIV (E = S, Se) with elemental sulfur and selenium: synthesis of polychalcogenido-bridged uranium complexes
• Authors of publication: Franke, Sebastian M.; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Chemical Science
• Year of publication: 2014
• Journal volume: 5
• Journal issue: 3
• Pages of publication: 942
• a: 18.092 ± 0.002 Å
• b: 12.365 ± 0.0006 Å
• c: 28.315 ± 0.003 Å
• α: 90 ± 0.007°
• β: 118.117 ± 0.012°
• γ: 90 ± 0.008°
• Cell volume: 5586.8 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0711
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections included in the refinement: 0.0802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.573
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No