Information card for entry 1516135

Structure parameters

• Formula: C14 H25 N O2 S Sn
• Calculated formula: C14 H25 N O2 S Sn
• SMILES: [Sn]([C@@H](NS(=O)(=O)C(C)(C)C)c1ccccc1)(C)(C)C
• Title of publication: Catalytic Enantioselective Silylation of N-Sulfonylimines: Asymmetric Synthesis of α-Amino Acids from CO2 via Stereospecific Carboxylation of α-Amino Silanes.
• Authors of publication: Mita, Tsuyoshi; Sugawara, Masumi; Saito, Keisuke; Sato, Yoshihiro
• Journal of publication: Organic letters
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 11
• Pages of publication: 3028 - 3031
• a: 11.1188 ± 0.0003 Å
• b: 10.5531 ± 0.0003 Å
• c: 15.6491 ± 0.0005 Å
• α: 90°
• β: 110.738 ± 0.008°
• γ: 90°
• Cell volume: 1717.26 ± 0.13 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.017
• Weighted residual factors for all reflections included in the refinement: 0.0434
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No