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Information card for entry 1517236
Preview
Coordinates | 1517236.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C14 H13 N O5 |
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Calculated formula | C14 H13 N O5 |
SMILES | O=C1O[C@@H](c2ccccc2)[C@H]2[C@@]1(NC(=O)C2)C(=O)OC.O=C1O[C@H](c2ccccc2)[C@@H]2[C@]1(NC(=O)C2)C(=O)OC |
Title of publication | Diastereoselective synthesis of fused lactone-pyrrolidinones; application to a formal synthesis of (-)-salinosporamide a. |
Authors of publication | Logan, Angus W. J.; Sprague, Simon J.; Foster, Robert W.; Marx, Léo B; Garzya, Vincenzo; Hallside, Michal S.; Thompson, Amber L.; Burton, Jonathan W. |
Journal of publication | Organic letters |
Year of publication | 2014 |
Journal volume | 16 |
Journal issue | 16 |
Pages of publication | 4078 - 4081 |
a | 6.9386 ± 0.0001 Å |
b | 15.1121 ± 0.0002 Å |
c | 23.6998 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2485.09 ± 0.06 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0482 |
Residual factor for significantly intense reflections | 0.0358 |
Weighted residual factors for all reflections | 0.0788 |
Weighted residual factors for significantly intense reflections | 0.0663 |
Weighted residual factors for all reflections included in the refinement | 0.0788 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9815 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1517236.html
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