Information card for entry 1517237

Structure parameters

• Formula: C26 H35 N O6
• Calculated formula: C26 H35 N O6
• SMILES: N1(C(=O)[C@@H]2[C@@H](C1(C(=O)OC(C)(C)C)C(=O)OC(C)(C)C)CC=CC2)Cc1ccc(cc1)OC
• Title of publication: Diastereoselective synthesis of fused lactone-pyrrolidinones; application to a formal synthesis of (-)-salinosporamide a.
• Authors of publication: Logan, Angus W. J.; Sprague, Simon J.; Foster, Robert W.; Marx, Léo B; Garzya, Vincenzo; Hallside, Michal S.; Thompson, Amber L.; Burton, Jonathan W.
• Journal of publication: Organic letters
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 16
• Pages of publication: 4078 - 4081
• a: 6.2769 ± 0.0001 Å
• b: 19.0465 ± 0.0002 Å
• c: 20.3494 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2432.83 ± 0.07 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for all reflections: 0.0999
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.0999
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9344
• Diffraction radiation wavelength: 0.6889 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No