Information card for entry 1517764

Structure parameters

• Formula: C52 H38 Cl4 N2 O4 P2 Pd
• Calculated formula: C50 H38 N2 O4 P2 Pd
• Title of publication: Monoanionic salicylaldimine ligands with (thio)phosphoryl pendant arms: Synthesis and complexing features
• Authors of publication: Diana V. Aleksanyan; Valentina Yu. Aleksenko; Yulia V. Nelyubina; Andrei A. Vasil-ev; Rinat R. Aysin; Zinaida S. Klemenkova; Vladimir A. Kozlov; Pavel V. Petrovskii; Irina L. Odinets
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 404
• Pages of publication: 167 - 174
• a: 8.3886 ± 0.0015 Å
• b: 11.599 ± 0.002 Å
• c: 14.078 ± 0.004 Å
• α: 105.217 ± 0.005°
• β: 105.536 ± 0.005°
• γ: 106.086 ± 0.004°
• Cell volume: 1181.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0952
• Weighted residual factors for all reflections included in the refinement: 0.1022
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No