Information card for entry 1517765

Structure parameters

• Formula: C27 H22 Cl N2 O P Pd S
• Calculated formula: C27 H22 Cl N2 O P Pd S
• Title of publication: Monoanionic salicylaldimine ligands with (thio)phosphoryl pendant arms: Synthesis and complexing features
• Authors of publication: Diana V. Aleksanyan; Valentina Yu. Aleksenko; Yulia V. Nelyubina; Andrei A. Vasil-ev; Rinat R. Aysin; Zinaida S. Klemenkova; Vladimir A. Kozlov; Pavel V. Petrovskii; Irina L. Odinets
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 404
• Pages of publication: 167 - 174
• a: 28.7944 ± 0.0018 Å
• b: 9.7914 ± 0.0006 Å
• c: 18.0302 ± 0.0011 Å
• α: 90°
• β: 100.461 ± 0.001°
• γ: 90°
• Cell volume: 4998.9 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1
• Weighted residual factors for all reflections included in the refinement: 0.1157
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No